Abstract

Title Fabrication and Properties of Si3N4 Fiber Material in a novel Method
Thematic area Energy Saving and Insulation
Presenter Prof. Wang Gang
Authors Prof. Wang Gang, Sinosteel Corporation Luoyang Institute of Refractory Research Co., Ltd., Luoyang - China
Mr. Han Jianshen, Sinosteel Corporation Luoyang Institute of Refractory Research Co., Ltd., Luoyang - China
Dr. Yuan Bo, Sinosteel Corporation Luoyang Institute of Refractory Research Co., Ltd., Luoyang - China
Mr. Dong Binbin, Sinosteel Corporation Luoyang Institute of Refractory Research Co., Ltd., Luoyang - China
Mr. Chen Kuo, Sinosteel Corporation Luoyang Institute of Refractory Research Co., Ltd., Luoyang - China
Prof. Li Hongxia, Sinosteel Corporation Luoyang Institute of Refractory Research Co., Ltd., Luoyang - China
Abstract

In this paper, Low-cost Si3N4 fiber material was synthesized by heating silicon porous body prepared via direct foaming method at 1400°C for 5h in a flowing N2 atmosphere. The influence of addition of foaming agent on the properties of Si3N4 fiber material was studied. The results showed that with the addition of foaming agent increased from 1 wt % to 4 wt %, the bulk density of Si3N4 fiber material reduced from 0.76 g/cm3 to 0.37 g/cm3, the compressive strength reduced from 6.1 Mpa to 1.6 Mpa and the thermal conductivity at 1000°C descended from 0.494 W·M-1·K-1 to 0.216 W·M-1·K-1. After staying in the cryolite steam at 1000°C for 50h, the properties of Si3N4 fiber material changed little. These indicate that Si3N4 fiber material has excellent thermal insulating performance and erosion resistance.

Key Words: Si3N4 fiber; porous; nitride; thermal insulation